Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES)
Resumen:
An analytical method for sample preparation of igneous rocks and subsequent determination of Si, Na, K, Ca, Mg, Al, Fe, Mn, Ba, Sr, and Ti by means of microwave induced emission spectrometry (MP-AES) was developed and validated. The proposed sample preparation procedure avoids the use of perchloric acid and provided accurate results even for silicon determination using an acid digestion with hydrofluoric acid. The determination of major elements in rocks is required for the design of classification diagrams that provides relevant information for geochemical analysis. • MP-AES showed to be an adequate technique to measure major and some trace elements that are relevant for classification of igneous rocks. • This method is in better agreement with the principles of the Green Analytical Chemistry and constitutes a reliable alternative to classical analytical and tedious procedures used for geochemical analysis. • The methodology was successfully applied to chemical classification of rocks from Valle Chico (Uruguay) using a Total Alkali-Silica Diagram (TAS).
| 2022 | |
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QUIMICA ANALITICA QUIMICA ANALITICA VERDE ESPECTROMETRIA ROCAS MP-AES |
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| Inglés | |
| Universidad de la República | |
| COLIBRI | |
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https://hdl.handle.net/20.500.12008/41357
https://doi.org/10.1016/j.mex.2022.101793 |
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| Acceso abierto | |
| Licencia Creative Commons Atribución (CC - By 4.0) |
| _version_ | 1875693325016629248 |
|---|---|
| author | Geisenblosen, María Cecilia |
| author2 | Oyhantçabal, Pedro Pistón, Mariela |
| author2_role | author author |
| author_facet | Geisenblosen, María Cecilia Oyhantçabal, Pedro Pistón, Mariela |
| author_role | author |
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| collection | COLIBRI |
| dc.contributor.filiacion.none.fl_str_mv | Geisenblosen María Cecilia, Ministerio de Industria Energía y Minería (Uruguay). Dirección Nacional de Minería y Geología; Universidad de la República (Uruguay). Facultad de Química, Graduate Program in Chemistry Oyhantçabal Pedro, Universidad de la República (Uruguay). Facultad de Ciencias, Instituto de Ciencias Geológicas, Departamento de Geodinámica Interna Pistón Mariela, Universidad de la República (Uruguay). Facultad de Química, DEC, Analytical Chemistry, Grupo de Análisis de Elementos Traza y Desarrollo de Estrategias Simples para Preparación de Muestras (GATPREM) |
| dc.creator.none.fl_str_mv | Geisenblosen, María Cecilia Oyhantçabal, Pedro Pistón, Mariela |
| dc.date.accessioned.none.fl_str_mv | 2023-11-21T11:53:49Z |
| dc.date.available.none.fl_str_mv | 2023-11-21T11:53:49Z |
| dc.date.issued.none.fl_str_mv | 2022 |
| dc.description.abstract.none.fl_txt_mv | An analytical method for sample preparation of igneous rocks and subsequent determination of Si, Na, K, Ca, Mg, Al, Fe, Mn, Ba, Sr, and Ti by means of microwave induced emission spectrometry (MP-AES) was developed and validated. The proposed sample preparation procedure avoids the use of perchloric acid and provided accurate results even for silicon determination using an acid digestion with hydrofluoric acid. The determination of major elements in rocks is required for the design of classification diagrams that provides relevant information for geochemical analysis. • MP-AES showed to be an adequate technique to measure major and some trace elements that are relevant for classification of igneous rocks. • This method is in better agreement with the principles of the Green Analytical Chemistry and constitutes a reliable alternative to classical analytical and tedious procedures used for geochemical analysis. • The methodology was successfully applied to chemical classification of rocks from Valle Chico (Uruguay) using a Total Alkali-Silica Diagram (TAS). |
| dc.format.mimetype.es.fl_str_mv | application/pdf |
| dc.identifier.citation.es.fl_str_mv | Geisenblosen, M, Oyhantçabal, P y Pistón, M. "Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES)". MethodsX. [en línea] 2022, vol. 9, e101793. DOI: https://doi.org/10.1016/j.mex.2022.101793 |
| dc.identifier.doi.none.fl_str_mv | https://doi.org/10.1016/j.mex.2022.101793 |
| dc.identifier.uri.none.fl_str_mv | https://hdl.handle.net/20.500.12008/41357 |
| dc.language.iso.none.fl_str_mv | en eng |
| dc.publisher.es.fl_str_mv | Elsevier |
| dc.relation.none.fl_str_mv | MethodsX v.9, 2022. -- e101793 |
| dc.rights.license.none.fl_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
| dc.rights.none.fl_str_mv | info:eu-repo/semantics/openAccess |
| dc.source.none.fl_str_mv | reponame:COLIBRI instname:Universidad de la República instacron:Universidad de la República |
| dc.subject.other.es.fl_str_mv | QUIMICA ANALITICA QUIMICA ANALITICA VERDE ESPECTROMETRIA ROCAS MP-AES |
| dc.title.none.fl_str_mv | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| dc.type.es.fl_str_mv | Artículo |
| dc.type.none.fl_str_mv | info:eu-repo/semantics/article |
| dc.type.version.none.fl_str_mv | info:eu-repo/semantics/publishedVersion |
| description | An analytical method for sample preparation of igneous rocks and subsequent determination of Si, Na, K, Ca, Mg, Al, Fe, Mn, Ba, Sr, and Ti by means of microwave induced emission spectrometry (MP-AES) was developed and validated. The proposed sample preparation procedure avoids the use of perchloric acid and provided accurate results even for silicon determination using an acid digestion with hydrofluoric acid. The determination of major elements in rocks is required for the design of classification diagrams that provides relevant information for geochemical analysis. • MP-AES showed to be an adequate technique to measure major and some trace elements that are relevant for classification of igneous rocks. • This method is in better agreement with the principles of the Green Analytical Chemistry and constitutes a reliable alternative to classical analytical and tedious procedures used for geochemical analysis. • The methodology was successfully applied to chemical classification of rocks from Valle Chico (Uruguay) using a Total Alkali-Silica Diagram (TAS). |
| eu_rights_str_mv | openAccess |
| format | article |
| id | COLIBRI_fea2e67dc7279c032d2b225eaff770e4 |
| identifier_str_mv | Geisenblosen, M, Oyhantçabal, P y Pistón, M. "Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES)". MethodsX. [en línea] 2022, vol. 9, e101793. DOI: https://doi.org/10.1016/j.mex.2022.101793 |
| instacron_str | Universidad de la República |
| institution | Universidad de la República |
| instname_str | Universidad de la República |
| language | eng |
| language_invalid_str_mv | en |
| network_acronym_str | COLIBRI |
| network_name_str | COLIBRI |
| oai_identifier_str | oai:colibri.udelar.edu.uy:20.500.12008/41357 |
| publishDate | 2022 |
| reponame_str | COLIBRI |
| repository.mail.fl_str_mv | karina.camps@seciu.edu.uy |
| repository.name.fl_str_mv | COLIBRI - Universidad de la República |
| repository_id_str | 4771 |
| rights_invalid_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
| spelling | Geisenblosen María Cecilia, Ministerio de Industria Energía y Minería (Uruguay). Dirección Nacional de Minería y Geología; Universidad de la República (Uruguay). Facultad de Química, Graduate Program in ChemistryOyhantçabal Pedro, Universidad de la República (Uruguay). Facultad de Ciencias, Instituto de Ciencias Geológicas, Departamento de Geodinámica InternaPistón Mariela, Universidad de la República (Uruguay). Facultad de Química, DEC, Analytical Chemistry, Grupo de Análisis de Elementos Traza y Desarrollo de Estrategias Simples para Preparación de Muestras (GATPREM)2023-11-21T11:53:49Z2023-11-21T11:53:49Z2022Geisenblosen, M, Oyhantçabal, P y Pistón, M. "Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES)". MethodsX. [en línea] 2022, vol. 9, e101793. DOI: https://doi.org/10.1016/j.mex.2022.101793https://hdl.handle.net/20.500.12008/41357https://doi.org/10.1016/j.mex.2022.101793An analytical method for sample preparation of igneous rocks and subsequent determination of Si, Na, K, Ca, Mg, Al, Fe, Mn, Ba, Sr, and Ti by means of microwave induced emission spectrometry (MP-AES) was developed and validated. The proposed sample preparation procedure avoids the use of perchloric acid and provided accurate results even for silicon determination using an acid digestion with hydrofluoric acid. The determination of major elements in rocks is required for the design of classification diagrams that provides relevant information for geochemical analysis. • MP-AES showed to be an adequate technique to measure major and some trace elements that are relevant for classification of igneous rocks. • This method is in better agreement with the principles of the Green Analytical Chemistry and constitutes a reliable alternative to classical analytical and tedious procedures used for geochemical analysis. • The methodology was successfully applied to chemical classification of rocks from Valle Chico (Uruguay) using a Total Alkali-Silica Diagram (TAS).Submitted by Silvana González (sgz@adinet.com.uy) on 2023-11-20T21:32:33Z No. of bitstreams: 2 license_rdf: 24251 bytes, checksum: 71ed42ef0a0b648670f707320be37b90 (MD5) AA Geisenblosen, M. MethodsX v.9, 2022. -- e101793.pdf: 889836 bytes, checksum: a0821301712504d6e3010c512dd39879 (MD5)Made available in DSpace by Luna Fabiana (fabiana.luna@seciu.edu.uy) on 2023-11-21T11:53:49Z (GMT). No. of bitstreams: 2 license_rdf: 24251 bytes, checksum: 71ed42ef0a0b648670f707320be37b90 (MD5) AA Geisenblosen, M. MethodsX v.9, 2022. -- e101793.pdf: 889836 bytes, checksum: a0821301712504d6e3010c512dd39879 (MD5) Previous issue date: 2022application/pdfenengElsevierMethodsX v.9, 2022. -- e101793Las obras depositadas en el Repositorio se rigen por la Ordenanza de los Derechos de la Propiedad Intelectual de la Universidad de la República.(Res. Nº 91 de C.D.C. de 8/III/1994 – D.O. 7/IV/1994) y por la Ordenanza del Repositorio Abierto de la Universidad de la República (Res. Nº 16 de C.D.C. de 07/10/2014)info:eu-repo/semantics/openAccessLicencia Creative Commons Atribución (CC - By 4.0)QUIMICA ANALITICAQUIMICA ANALITICA VERDEESPECTROMETRIAROCASMP-AESDetermination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES)Artículoinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionreponame:COLIBRIinstname:Universidad de la Repúblicainstacron:Universidad de la RepúblicaGeisenblosen, María CeciliaOyhantçabal, PedroPistón, MarielaLICENSElicense.txtlicense.txttext/plain; charset=utf-84267http://localhost:8080/xmlui/bitstream/20.500.12008/41357/5/license.txt6429389a7df7277b72b7924fdc7d47a9MD55CC-LICENSElicense_urllicense_urltext/plain; charset=utf-844http://localhost:8080/xmlui/bitstream/20.500.12008/41357/2/license_urla0ebbeafb9d2ec7cbb19d7137ebc392cMD52license_textlicense_texttext/html; charset=utf-813786http://localhost:8080/xmlui/bitstream/20.500.12008/41357/3/license_text9b2f65dcc322aef148d393163faed91bMD53license_rdflicense_rdfapplication/rdf+xml; charset=utf-824251http://localhost:8080/xmlui/bitstream/20.500.12008/41357/4/license_rdf71ed42ef0a0b648670f707320be37b90MD54ORIGINALAA Geisenblosen, M. MethodsX v.9, 2022. -- e101793.pdfAA Geisenblosen, M. 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- Universidad de la Repúblicafalse |
| spellingShingle | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) Geisenblosen, María Cecilia QUIMICA ANALITICA QUIMICA ANALITICA VERDE ESPECTROMETRIA ROCAS MP-AES |
| status_str | publishedVersion |
| title | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| title_full | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| title_fullStr | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| title_full_unstemmed | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| title_short | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| title_sort | Determination of major elements in igneous rocks using microwave plasma atomic emission spectrometry (MP-AES) |
| topic | QUIMICA ANALITICA QUIMICA ANALITICA VERDE ESPECTROMETRIA ROCAS MP-AES |
| url | https://hdl.handle.net/20.500.12008/41357 https://doi.org/10.1016/j.mex.2022.101793 |
