In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite
Resumen:
A time resolved in situ X-ray powder diffraction study using synchrotron radiation allowed for describing the evolution of the zeolite FAU structure during the development of a zeolitetemplated carbon (ZTC) in its porous voids. During the ZTC formation the intensity decrease of most zeolite reflections and the simultaneous rise in intensity of the 222 reflection (of null intensity in the pristine zeolite) was observed. Full pattern profile fitting by Rietveld refinement allowed for achieving a detailed description of the underlying chemistry, with coincident pore filling with carbon atoms in specific positions and framework distortion. Monitoring the intensity profiles of the 222 reflection allowed assessment of the energetics of the ZTC formation. Our results contribute to a better understanding of the phenomena involved on the atomic scale in ZTC synthesis.
| 2024 | |
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ZEOLITAS DIFRACCION DE RAYOS X |
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| Inglés | |
| Universidad de la República | |
| COLIBRI | |
| https://hdl.handle.net/20.500.12008/47492 | |
| Acceso abierto | |
| Licencia Creative Commons Atribución (CC - By 4.0) |
| _version_ | 1877555085746110464 |
|---|---|
| author | Amound, Thibaud |
| author2 | Esteves, Martin Mocuta, Cristian Batonneau-Gener, Isabelle Haines, Julien Faccio, Ricardo Sachse, Alexander |
| author2_role | author author author author author author |
| author_facet | Amound, Thibaud Esteves, Martin Mocuta, Cristian Batonneau-Gener, Isabelle Haines, Julien Faccio, Ricardo Sachse, Alexander |
| author_role | author |
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| collection | COLIBRI |
| dc.contributor.filiacion.none.fl_str_mv | Amound Thibaud, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 7285 Esteves Martin, Universidad de la República (Uruguay). Departamento de Experimentación y Teoría de la Estructura de la Materia y sus Aplicaciones (DETEMA). Centro NanoMat y Área Física Mocuta Cristian, Synchrotron SOLEIL (Francia) Batonneau-Gener Isabelle, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 7285 Haines Julien, Université de Montpellier (Francia). Institut Charles Gerhardt Montpellier Faccio Ricardo, Universidad de la República (Uruguay). Departamento de Experimentación y Teoría de la Estructura de la Materia y sus Aplicaciones (DETEMA). Centro NanoMat y Área Física Sachse Alexander, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 7285 |
| dc.creator.none.fl_str_mv | Amound, Thibaud Esteves, Martin Mocuta, Cristian Batonneau-Gener, Isabelle Haines, Julien Faccio, Ricardo Sachse, Alexander |
| dc.date.accessioned.none.fl_str_mv | 2024-12-11T18:03:01Z |
| dc.date.available.none.fl_str_mv | 2024-12-11T18:03:01Z |
| dc.date.issued.none.fl_str_mv | 2024 |
| dc.description.abstract.none.fl_txt_mv | A time resolved in situ X-ray powder diffraction study using synchrotron radiation allowed for describing the evolution of the zeolite FAU structure during the development of a zeolitetemplated carbon (ZTC) in its porous voids. During the ZTC formation the intensity decrease of most zeolite reflections and the simultaneous rise in intensity of the 222 reflection (of null intensity in the pristine zeolite) was observed. Full pattern profile fitting by Rietveld refinement allowed for achieving a detailed description of the underlying chemistry, with coincident pore filling with carbon atoms in specific positions and framework distortion. Monitoring the intensity profiles of the 222 reflection allowed assessment of the energetics of the ZTC formation. Our results contribute to a better understanding of the phenomena involved on the atomic scale in ZTC synthesis. |
| dc.format.extent.es.fl_str_mv | 6 p. |
| dc.format.mimetype.es.fl_str_mv | application/pdf |
| dc.identifier.citation.es.fl_str_mv | Amound, T., Esteves, M., Mocuta, C. y otros. "In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite". Chemistry-Methods [en línea] 2024. -- e202400018. 6 p. |
| dc.identifier.doi.none.fl_str_mv | 10.1002/cmtd.202400018 |
| dc.identifier.uri.none.fl_str_mv | https://hdl.handle.net/20.500.12008/47492 |
| dc.language.iso.none.fl_str_mv | en eng |
| dc.publisher.es.fl_str_mv | Wiley |
| dc.relation.none.fl_str_mv | PDF Chemistry-Methods, 2024. -- e202400018 |
| dc.rights.license.none.fl_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
| dc.rights.none.fl_str_mv | info:eu-repo/semantics/openAccess |
| dc.source.none.fl_str_mv | reponame:COLIBRI instname:Universidad de la República instacron:Universidad de la República |
| dc.subject.other.es.fl_str_mv | ZEOLITAS DIFRACCION DE RAYOS X |
| dc.title.none.fl_str_mv | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| dc.type.es.fl_str_mv | Artículo |
| dc.type.none.fl_str_mv | info:eu-repo/semantics/article |
| dc.type.version.none.fl_str_mv | info:eu-repo/semantics/publishedVersion |
| description | A time resolved in situ X-ray powder diffraction study using synchrotron radiation allowed for describing the evolution of the zeolite FAU structure during the development of a zeolitetemplated carbon (ZTC) in its porous voids. During the ZTC formation the intensity decrease of most zeolite reflections and the simultaneous rise in intensity of the 222 reflection (of null intensity in the pristine zeolite) was observed. Full pattern profile fitting by Rietveld refinement allowed for achieving a detailed description of the underlying chemistry, with coincident pore filling with carbon atoms in specific positions and framework distortion. Monitoring the intensity profiles of the 222 reflection allowed assessment of the energetics of the ZTC formation. Our results contribute to a better understanding of the phenomena involved on the atomic scale in ZTC synthesis. |
| eu_rights_str_mv | openAccess |
| format | article |
| id | COLIBRI_bd2a9746d7b1e26b1d7914b30ffef007 |
| identifier_str_mv | Amound, T., Esteves, M., Mocuta, C. y otros. "In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite". Chemistry-Methods [en línea] 2024. -- e202400018. 6 p. 10.1002/cmtd.202400018 |
| instacron_str | Universidad de la República |
| institution | Universidad de la República |
| instname_str | Universidad de la República |
| language | eng |
| language_invalid_str_mv | en |
| network_acronym_str | COLIBRI |
| network_name_str | COLIBRI |
| oai_identifier_str | oai:colibri.udelar.edu.uy:20.500.12008/47492 |
| publishDate | 2024 |
| reponame_str | COLIBRI |
| repository.mail.fl_str_mv | karina.camps@seciu.edu.uy |
| repository.name.fl_str_mv | COLIBRI - Universidad de la República |
| repository_id_str | 4771 |
| rights_invalid_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
| spelling | Amound Thibaud, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 7285Esteves Martin, Universidad de la República (Uruguay). Departamento de Experimentación y Teoría de la Estructura de la Materia y sus Aplicaciones (DETEMA). Centro NanoMat y Área FísicaMocuta Cristian, Synchrotron SOLEIL (Francia)Batonneau-Gener Isabelle, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 7285Haines Julien, Université de Montpellier (Francia). Institut Charles Gerhardt MontpellierFaccio Ricardo, Universidad de la República (Uruguay). Departamento de Experimentación y Teoría de la Estructura de la Materia y sus Aplicaciones (DETEMA). Centro NanoMat y Área FísicaSachse Alexander, Université de Poitiers (Francia). CNRS. Institut de Chimie des Milieux et Matériaux de Poitiers (IC2MP) - UMR 72852024-12-11T18:03:01Z2024-12-11T18:03:01Z2024Amound, T., Esteves, M., Mocuta, C. y otros. "In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite". Chemistry-Methods [en línea] 2024. -- e202400018. 6 p.https://hdl.handle.net/20.500.12008/4749210.1002/cmtd.202400018A time resolved in situ X-ray powder diffraction study using synchrotron radiation allowed for describing the evolution of the zeolite FAU structure during the development of a zeolitetemplated carbon (ZTC) in its porous voids. During the ZTC formation the intensity decrease of most zeolite reflections and the simultaneous rise in intensity of the 222 reflection (of null intensity in the pristine zeolite) was observed. Full pattern profile fitting by Rietveld refinement allowed for achieving a detailed description of the underlying chemistry, with coincident pore filling with carbon atoms in specific positions and framework distortion. Monitoring the intensity profiles of the 222 reflection allowed assessment of the energetics of the ZTC formation. Our results contribute to a better understanding of the phenomena involved on the atomic scale in ZTC synthesis.Submitted by Suhr Deborah (dsuhr@fq.edu.uy) on 2024-12-10T17:08:38Z No. of bitstreams: 2 license_rdf: 24251 bytes, checksum: 71ed42ef0a0b648670f707320be37b90 (MD5) In situ X-Ray Powder.pdf: 8007817 bytes, checksum: e6c3c8bca95294df6348e28542e134f4 (MD5)Made available in DSpace by Luna Fabiana (fabiana.luna@seciu.edu.uy) on 2024-12-11T18:03:01Z (GMT). No. of bitstreams: 2 license_rdf: 24251 bytes, checksum: 71ed42ef0a0b648670f707320be37b90 (MD5) In situ X-Ray Powder.pdf: 8007817 bytes, checksum: e6c3c8bca95294df6348e28542e134f4 (MD5) Previous issue date: 20246 p.application/pdfenengWileyPDFChemistry-Methods, 2024. -- e202400018Las obras depositadas en el Repositorio se rigen por la Ordenanza de los Derechos de la Propiedad Intelectual de la Universidad de la República.(Res. Nº 91 de C.D.C. de 8/III/1994 – D.O. 7/IV/1994) y por la Ordenanza del Repositorio Abierto de la Universidad de la República (Res. Nº 16 de C.D.C. de 07/10/2014)info:eu-repo/semantics/openAccessLicencia Creative Commons Atribución (CC - By 4.0)ZEOLITASDIFRACCION DE RAYOS XIn situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeoliteArtículoinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionreponame:COLIBRIinstname:Universidad de la Repúblicainstacron:Universidad de la RepúblicaAmound, ThibaudEsteves, MartinMocuta, CristianBatonneau-Gener, IsabelleHaines, JulienFaccio, RicardoSachse, AlexanderLICENSElicense.txtlicense.txttext/plain; charset=utf-84267http://localhost:8080/xmlui/bitstream/20.500.12008/47492/5/license.txt6429389a7df7277b72b7924fdc7d47a9MD55CC-LICENSElicense_urllicense_urltext/plain; charset=utf-844http://localhost:8080/xmlui/bitstream/20.500.12008/47492/2/license_urla0ebbeafb9d2ec7cbb19d7137ebc392cMD52license_textlicense_texttext/html; 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- Universidad de la Repúblicafalse |
| spellingShingle | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite Amound, Thibaud ZEOLITAS DIFRACCION DE RAYOS X |
| status_str | publishedVersion |
| title | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| title_full | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| title_fullStr | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| title_full_unstemmed | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| title_short | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| title_sort | In situ x-ray powder diffraction investigation on the development of zeolite-templated carbons in FAU zeolite |
| topic | ZEOLITAS DIFRACCION DE RAYOS X |
| url | https://hdl.handle.net/20.500.12008/47492 |
