Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
Resumen:
High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant
2019 | |
Ceramic blocks Bone graft Bovine bone Biomaterials Cellular analysis |
|
Inglés | |
Universidad de la República | |
COLIBRI | |
https://hdl.handle.net/20.500.12008/28669 | |
Acceso abierto | |
Licencia Creative Commons Atribución (CC - By 4.0) |
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author | Gehrke, S.A. |
author2 | Mazón, P. Pérez-Díaz, Leticia Calvo-Guirado, J.L. Velásquez, P. Aragoneses, J.M. Fernández-Domínguez, M. De Aza, P.N. |
author2_role | author author author author author author author |
author_facet | Gehrke, S.A. Mazón, P. Pérez-Díaz, Leticia Calvo-Guirado, J.L. Velásquez, P. Aragoneses, J.M. Fernández-Domínguez, M. De Aza, P.N. |
author_role | author |
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bitstream.checksumAlgorithm.fl_str_mv | MD5 MD5 MD5 MD5 MD5 |
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collection | COLIBRI |
dc.contributor.filiacion.none.fl_str_mv | Gehrke S.A. Mazón P. Pérez-Díaz Leticia, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Química Biológica. Calvo-Guirado J.L. Velásquez P. Aragoneses J.M. Fernández-Domínguez M. De Aza P.N. |
dc.creator.none.fl_str_mv | Gehrke, S.A. Mazón, P. Pérez-Díaz, Leticia Calvo-Guirado, J.L. Velásquez, P. Aragoneses, J.M. Fernández-Domínguez, M. De Aza, P.N. |
dc.date.accessioned.none.fl_str_mv | 2021-07-22T13:12:19Z |
dc.date.available.none.fl_str_mv | 2021-07-22T13:12:19Z |
dc.date.issued.none.fl_str_mv | 2019 |
dc.description.abstract.none.fl_txt_mv | High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant |
dc.format.extent.es.fl_str_mv | 18 h. |
dc.format.mimetype.es.fl_str_mv | application/pdf |
dc.identifier.citation.es.fl_str_mv | Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma12030452 |
dc.identifier.doi.none.fl_str_mv | 10.3390/ma12030452 |
dc.identifier.issn.none.fl_str_mv | 1996-1944 |
dc.identifier.uri.none.fl_str_mv | https://hdl.handle.net/20.500.12008/28669 |
dc.language.iso.none.fl_str_mv | en eng |
dc.publisher.es.fl_str_mv | MDPI |
dc.relation.ispartof.es.fl_str_mv | Materials, 2019, 12(3):452 |
dc.rights.license.none.fl_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
dc.rights.none.fl_str_mv | info:eu-repo/semantics/openAccess |
dc.source.none.fl_str_mv | reponame:COLIBRI instname:Universidad de la República instacron:Universidad de la República |
dc.subject.en.fl_str_mv | Ceramic blocks Bone graft Bovine bone Biomaterials Cellular analysis |
dc.title.none.fl_str_mv | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
dc.type.es.fl_str_mv | Artículo |
dc.type.none.fl_str_mv | info:eu-repo/semantics/article |
dc.type.version.none.fl_str_mv | info:eu-repo/semantics/publishedVersion |
description | High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant |
eu_rights_str_mv | openAccess |
format | article |
id | COLIBRI_84b7f0350af94f4bf55ae9f8d0a22d41 |
identifier_str_mv | Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma12030452 1996-1944 10.3390/ma12030452 |
instacron_str | Universidad de la República |
institution | Universidad de la República |
instname_str | Universidad de la República |
language | eng |
language_invalid_str_mv | en |
network_acronym_str | COLIBRI |
network_name_str | COLIBRI |
oai_identifier_str | oai:colibri.udelar.edu.uy:20.500.12008/28669 |
publishDate | 2019 |
reponame_str | COLIBRI |
repository.mail.fl_str_mv | mabel.seroubian@seciu.edu.uy |
repository.name.fl_str_mv | COLIBRI - Universidad de la República |
repository_id_str | 4771 |
rights_invalid_str_mv | Licencia Creative Commons Atribución (CC - By 4.0) |
spelling | Gehrke S.A.Mazón P.Pérez-Díaz Leticia, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Química Biológica.Calvo-Guirado J.L.Velásquez P.Aragoneses J.M.Fernández-Domínguez M.De Aza P.N.2021-07-22T13:12:19Z2021-07-22T13:12:19Z2019Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma120304521996-1944https://hdl.handle.net/20.500.12008/2866910.3390/ma12030452High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominantSubmitted by Verdun Juan Pablo (jverdun@fcien.edu.uy) on 2021-07-08T14:02:22Z No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5)Approved for entry into archive by Faget Cecilia (lfaget@fcien.edu.uy) on 2021-07-22T12:55:01Z (GMT) No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5)Made available in DSpace by Luna Fabiana (fabiana.luna@seciu.edu.uy) on 2021-07-22T13:12:19Z (GMT). No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5) Previous issue date: 201918 h.application/pdfenengMDPIMaterials, 2019, 12(3):452Las obras depositadas en el Repositorio se rigen por la Ordenanza de los Derechos de la Propiedad Intelectual de la Universidad de la República.(Res. Nº 91 de C.D.C. de 8/III/1994 – D.O. 7/IV/1994) y por la Ordenanza del Repositorio Abierto de la Universidad de la República (Res. Nº 16 de C.D.C. de 07/10/2014)info:eu-repo/semantics/openAccessLicencia Creative Commons Atribución (CC - By 4.0)Ceramic blocksBone graftBovine boneBiomaterialsCellular analysisStudy of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysisArtículoinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionreponame:COLIBRIinstname:Universidad de la Repúblicainstacron:Universidad de la RepúblicaGehrke, S.A.Mazón, P.Pérez-Díaz, LeticiaCalvo-Guirado, J.L.Velásquez, P.Aragoneses, J.M.Fernández-Domínguez, M.De Aza, P.N.LICENSElicense.txtlicense.txttext/plain; charset=utf-84267http://localhost:8080/xmlui/bitstream/20.500.12008/28669/5/license.txt6429389a7df7277b72b7924fdc7d47a9MD55CC-LICENSElicense_urllicense_urltext/plain; charset=utf-844http://localhost:8080/xmlui/bitstream/20.500.12008/28669/2/license_urla0ebbeafb9d2ec7cbb19d7137ebc392cMD52license_textlicense_texttext/html; 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- Universidad de la Repúblicafalse |
spellingShingle | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis Gehrke, S.A. Ceramic blocks Bone graft Bovine bone Biomaterials Cellular analysis |
status_str | publishedVersion |
title | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
title_full | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
title_fullStr | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
title_full_unstemmed | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
title_short | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
title_sort | Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis |
topic | Ceramic blocks Bone graft Bovine bone Biomaterials Cellular analysis |
url | https://hdl.handle.net/20.500.12008/28669 |