Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis

Gehrke, S.A. - Mazón, P. - Pérez-Díaz, Leticia - Calvo-Guirado, J.L. - Velásquez, P. - Aragoneses, J.M. - Fernández-Domínguez, M. - De Aza, P.N.

Resumen:

High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant


Detalles Bibliográficos
2019
Ceramic blocks
Bone graft
Bovine bone
Biomaterials
Cellular analysis
Inglés
Universidad de la República
COLIBRI
https://hdl.handle.net/20.500.12008/28669
Acceso abierto
Licencia Creative Commons Atribución (CC - By 4.0)
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author Gehrke, S.A.
author2 Mazón, P.
Pérez-Díaz, Leticia
Calvo-Guirado, J.L.
Velásquez, P.
Aragoneses, J.M.
Fernández-Domínguez, M.
De Aza, P.N.
author2_role author
author
author
author
author
author
author
author_facet Gehrke, S.A.
Mazón, P.
Pérez-Díaz, Leticia
Calvo-Guirado, J.L.
Velásquez, P.
Aragoneses, J.M.
Fernández-Domínguez, M.
De Aza, P.N.
author_role author
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collection COLIBRI
dc.contributor.filiacion.none.fl_str_mv Gehrke S.A.
Mazón P.
Pérez-Díaz Leticia, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Química Biológica.
Calvo-Guirado J.L.
Velásquez P.
Aragoneses J.M.
Fernández-Domínguez M.
De Aza P.N.
dc.creator.none.fl_str_mv Gehrke, S.A.
Mazón, P.
Pérez-Díaz, Leticia
Calvo-Guirado, J.L.
Velásquez, P.
Aragoneses, J.M.
Fernández-Domínguez, M.
De Aza, P.N.
dc.date.accessioned.none.fl_str_mv 2021-07-22T13:12:19Z
dc.date.available.none.fl_str_mv 2021-07-22T13:12:19Z
dc.date.issued.none.fl_str_mv 2019
dc.description.abstract.none.fl_txt_mv High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant
dc.format.extent.es.fl_str_mv 18 h.
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dc.identifier.citation.es.fl_str_mv Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma12030452
dc.identifier.doi.none.fl_str_mv 10.3390/ma12030452
dc.identifier.issn.none.fl_str_mv 1996-1944
dc.identifier.uri.none.fl_str_mv https://hdl.handle.net/20.500.12008/28669
dc.language.iso.none.fl_str_mv en
eng
dc.publisher.es.fl_str_mv MDPI
dc.relation.ispartof.es.fl_str_mv Materials, 2019, 12(3):452
dc.rights.license.none.fl_str_mv Licencia Creative Commons Atribución (CC - By 4.0)
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
dc.source.none.fl_str_mv reponame:COLIBRI
instname:Universidad de la República
instacron:Universidad de la República
dc.subject.en.fl_str_mv Ceramic blocks
Bone graft
Bovine bone
Biomaterials
Cellular analysis
dc.title.none.fl_str_mv Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
dc.type.es.fl_str_mv Artículo
dc.type.none.fl_str_mv info:eu-repo/semantics/article
dc.type.version.none.fl_str_mv info:eu-repo/semantics/publishedVersion
description High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant
eu_rights_str_mv openAccess
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identifier_str_mv Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma12030452
1996-1944
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publishDate 2019
reponame_str COLIBRI
repository.mail.fl_str_mv mabel.seroubian@seciu.edu.uy
repository.name.fl_str_mv COLIBRI - Universidad de la República
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rights_invalid_str_mv Licencia Creative Commons Atribución (CC - By 4.0)
spelling Gehrke S.A.Mazón P.Pérez-Díaz Leticia, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Química Biológica.Calvo-Guirado J.L.Velásquez P.Aragoneses J.M.Fernández-Domínguez M.De Aza P.N.2021-07-22T13:12:19Z2021-07-22T13:12:19Z2019Gehrke, S, Mazón, P, Pérez-Díaz, L, y otros "Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis". Materials. [en línea] 2019, 12(3): 452. 18 h. DOI: 10.3390/ma120304521996-1944https://hdl.handle.net/20.500.12008/2866910.3390/ma12030452High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominantSubmitted by Verdun Juan Pablo (jverdun@fcien.edu.uy) on 2021-07-08T14:02:22Z No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5)Approved for entry into archive by Faget Cecilia (lfaget@fcien.edu.uy) on 2021-07-22T12:55:01Z (GMT) No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5)Made available in DSpace by Luna Fabiana (fabiana.luna@seciu.edu.uy) on 2021-07-22T13:12:19Z (GMT). No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.3390ma12030452.pdf: 3297053 bytes, checksum: 6e5999866bbbaa084ab2589f7c4ba31c (MD5) Previous issue date: 201918 h.application/pdfenengMDPIMaterials, 2019, 12(3):452Las obras depositadas en el Repositorio se rigen por la Ordenanza de los Derechos de la Propiedad Intelectual de la Universidad de la República.(Res. Nº 91 de C.D.C. de 8/III/1994 – D.O. 7/IV/1994) y por la Ordenanza del Repositorio Abierto de la Universidad de la República (Res. Nº 16 de C.D.C. de 07/10/2014)info:eu-repo/semantics/openAccessLicencia Creative Commons Atribución (CC - By 4.0)Ceramic blocksBone graftBovine boneBiomaterialsCellular analysisStudy of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysisArtículoinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionreponame:COLIBRIinstname:Universidad de la Repúblicainstacron:Universidad de la RepúblicaGehrke, S.A.Mazón, P.Pérez-Díaz, LeticiaCalvo-Guirado, J.L.Velásquez, P.Aragoneses, J.M.Fernández-Domínguez, M.De Aza, P.N.LICENSElicense.txtlicense.txttext/plain; charset=utf-84267http://localhost:8080/xmlui/bitstream/20.500.12008/28669/5/license.txt6429389a7df7277b72b7924fdc7d47a9MD55CC-LICENSElicense_urllicense_urltext/plain; charset=utf-844http://localhost:8080/xmlui/bitstream/20.500.12008/28669/2/license_urla0ebbeafb9d2ec7cbb19d7137ebc392cMD52license_textlicense_texttext/html; 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- Universidad de la Repúblicafalse
spellingShingle Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
Gehrke, S.A.
Ceramic blocks
Bone graft
Bovine bone
Biomaterials
Cellular analysis
status_str publishedVersion
title Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
title_full Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
title_fullStr Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
title_full_unstemmed Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
title_short Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
title_sort Study of two bovine bone blocks (sintered and non-sintered) used for bone grafts: physico-chemical characterization and in vitro bioactivity and cellular analysis
topic Ceramic blocks
Bone graft
Bovine bone
Biomaterials
Cellular analysis
url https://hdl.handle.net/20.500.12008/28669