Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys

Moreno-Gobbi, Ariel - Silva, Paulo Sergio Jr. - Nespeque Correa, Diego Rafael - Masó Milá, Alfredo - Muños Chaves, Javier Andrés - Grandini, Carlos Roberto - Santos, Rafael Formenton Macedo dos - Moreira Afonso, Conrado Ramos

Resumen:

Ultrasonic velocity and attenuation measurements of a commercially available Ni-rich polycrystalline NieTi alloy were simultaneously obtained upon cooling from room temperature (RT) down to 130 K. The anelastic spectra show multiple anomalies in both velocity and attenuation curves, which evidence a complex nature of structural rearrangements exhibited by NieTi alloy, associated with relaxations and phase transformations. In particular, some evident anomalies at 285 and 180 K, not previously exploited using ultrasonic measurements on Ni-rich polycrystalline NieTi alloy, were associated with austenite to pre-martensitic (B2 / R) and pre-martensitic to martensitic (R/ B19’) phase transitions, respectively. The peculiar temperature separation between these transformations was interpreted based on chemical composition and the NieTi alloy microstructure evolution. X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC) were also used to add complementary results about phase transformations and thermal events exhibited by NieTi alloy at low temperatures.


Detalles Bibliográficos
2022
Ni-Ti alloy
Ultrasonic characterization
Martensitic transformations
Cryogenic temperature
Thermal properties
Inglés
Universidad de la República
COLIBRI
https://hdl.handle.net/20.500.12008/38531
Acceso abierto
Licencia Creative Commons Atribución (CC - By 4.0)
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author Moreno-Gobbi, Ariel
author2 Silva, Paulo Sergio Jr.
Nespeque Correa, Diego Rafael
Masó Milá, Alfredo
Muños Chaves, Javier Andrés
Grandini, Carlos Roberto
Santos, Rafael Formenton Macedo dos
Moreira Afonso, Conrado Ramos
author2_role author
author
author
author
author
author
author
author_facet Moreno-Gobbi, Ariel
Silva, Paulo Sergio Jr.
Nespeque Correa, Diego Rafael
Masó Milá, Alfredo
Muños Chaves, Javier Andrés
Grandini, Carlos Roberto
Santos, Rafael Formenton Macedo dos
Moreira Afonso, Conrado Ramos
author_role author
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collection COLIBRI
dc.contributor.filiacion.none.fl_str_mv Moreno-Gobbi Ariel, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Física.
Silva Paulo Sergio Jr.
Nespeque Correa Diego Rafael
Masó Milá Alfredo
Muños Chaves Javier Andrés
Grandini Carlos Roberto
Santos Rafael Formenton Macedo dos
Moreira Afonso Conrado Ramos
dc.creator.none.fl_str_mv Moreno-Gobbi, Ariel
Silva, Paulo Sergio Jr.
Nespeque Correa, Diego Rafael
Masó Milá, Alfredo
Muños Chaves, Javier Andrés
Grandini, Carlos Roberto
Santos, Rafael Formenton Macedo dos
Moreira Afonso, Conrado Ramos
dc.date.accessioned.none.fl_str_mv 2023-07-31T14:59:48Z
dc.date.available.none.fl_str_mv 2023-07-31T14:59:48Z
dc.date.issued.none.fl_str_mv 2022
dc.description.abstract.none.fl_txt_mv Ultrasonic velocity and attenuation measurements of a commercially available Ni-rich polycrystalline NieTi alloy were simultaneously obtained upon cooling from room temperature (RT) down to 130 K. The anelastic spectra show multiple anomalies in both velocity and attenuation curves, which evidence a complex nature of structural rearrangements exhibited by NieTi alloy, associated with relaxations and phase transformations. In particular, some evident anomalies at 285 and 180 K, not previously exploited using ultrasonic measurements on Ni-rich polycrystalline NieTi alloy, were associated with austenite to pre-martensitic (B2 / R) and pre-martensitic to martensitic (R/ B19’) phase transitions, respectively. The peculiar temperature separation between these transformations was interpreted based on chemical composition and the NieTi alloy microstructure evolution. X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC) were also used to add complementary results about phase transformations and thermal events exhibited by NieTi alloy at low temperatures.
dc.format.extent.es.fl_str_mv 15 h.
dc.format.mimetype.es.fl_str_mv application/pdf
dc.identifier.citation.es.fl_str_mv Moreno-Gobbi, A, Silva, P, Nespeque Correa, D, [y otros autores]. "Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys". Journal of Materials Research and Technology. [en línea] 2022, 18:4940-5004. 15 h. DOI: 10.1016/j.jmrt.2022.04.096
dc.identifier.doi.none.fl_str_mv 10.1016/j.jmrt.2022.04.096
dc.identifier.issn.none.fl_str_mv 22387854
dc.identifier.uri.none.fl_str_mv https://hdl.handle.net/20.500.12008/38531
dc.language.iso.none.fl_str_mv en_US
eng
dc.publisher.es.fl_str_mv Elsevier B.V
dc.relation.ispartof.es.fl_str_mv Journal of Materials Research and Technology, 2022, 18:4940-5004.
dc.rights.license.none.fl_str_mv Licencia Creative Commons Atribución (CC - By 4.0)
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
dc.source.none.fl_str_mv reponame:COLIBRI
instname:Universidad de la República
instacron:Universidad de la República
dc.subject.es.fl_str_mv Ni-Ti alloy
Ultrasonic characterization
Martensitic transformations
Cryogenic temperature
Thermal properties
dc.title.none.fl_str_mv Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
dc.type.es.fl_str_mv Artículo
dc.type.none.fl_str_mv info:eu-repo/semantics/article
dc.type.version.none.fl_str_mv info:eu-repo/semantics/publishedVersion
description Ultrasonic velocity and attenuation measurements of a commercially available Ni-rich polycrystalline NieTi alloy were simultaneously obtained upon cooling from room temperature (RT) down to 130 K. The anelastic spectra show multiple anomalies in both velocity and attenuation curves, which evidence a complex nature of structural rearrangements exhibited by NieTi alloy, associated with relaxations and phase transformations. In particular, some evident anomalies at 285 and 180 K, not previously exploited using ultrasonic measurements on Ni-rich polycrystalline NieTi alloy, were associated with austenite to pre-martensitic (B2 / R) and pre-martensitic to martensitic (R/ B19’) phase transitions, respectively. The peculiar temperature separation between these transformations was interpreted based on chemical composition and the NieTi alloy microstructure evolution. X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC) were also used to add complementary results about phase transformations and thermal events exhibited by NieTi alloy at low temperatures.
eu_rights_str_mv openAccess
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identifier_str_mv Moreno-Gobbi, A, Silva, P, Nespeque Correa, D, [y otros autores]. "Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys". Journal of Materials Research and Technology. [en línea] 2022, 18:4940-5004. 15 h. DOI: 10.1016/j.jmrt.2022.04.096
22387854
10.1016/j.jmrt.2022.04.096
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institution Universidad de la República
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language eng
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publishDate 2022
reponame_str COLIBRI
repository.mail.fl_str_mv mabel.seroubian@seciu.edu.uy
repository.name.fl_str_mv COLIBRI - Universidad de la República
repository_id_str 4771
rights_invalid_str_mv Licencia Creative Commons Atribución (CC - By 4.0)
spelling Moreno-Gobbi Ariel, Universidad de la República (Uruguay). Facultad de Ciencias. Instituto de Física.Silva Paulo Sergio Jr.Nespeque Correa Diego RafaelMasó Milá AlfredoMuños Chaves Javier AndrésGrandini Carlos RobertoSantos Rafael Formenton Macedo dosMoreira Afonso Conrado Ramos2023-07-31T14:59:48Z2023-07-31T14:59:48Z2022Moreno-Gobbi, A, Silva, P, Nespeque Correa, D, [y otros autores]. "Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys". Journal of Materials Research and Technology. [en línea] 2022, 18:4940-5004. 15 h. DOI: 10.1016/j.jmrt.2022.04.09622387854https://hdl.handle.net/20.500.12008/3853110.1016/j.jmrt.2022.04.096Ultrasonic velocity and attenuation measurements of a commercially available Ni-rich polycrystalline NieTi alloy were simultaneously obtained upon cooling from room temperature (RT) down to 130 K. The anelastic spectra show multiple anomalies in both velocity and attenuation curves, which evidence a complex nature of structural rearrangements exhibited by NieTi alloy, associated with relaxations and phase transformations. In particular, some evident anomalies at 285 and 180 K, not previously exploited using ultrasonic measurements on Ni-rich polycrystalline NieTi alloy, were associated with austenite to pre-martensitic (B2 / R) and pre-martensitic to martensitic (R/ B19’) phase transitions, respectively. The peculiar temperature separation between these transformations was interpreted based on chemical composition and the NieTi alloy microstructure evolution. X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC) were also used to add complementary results about phase transformations and thermal events exhibited by NieTi alloy at low temperatures.Submitted by Farías Verónica (vfarias@fcien.edu.uy) on 2023-07-31T14:27:59Z No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.1016jjmrt.202204096.pdf: 4557826 bytes, checksum: 4fdb91b90493c84f72eed099fe081737 (MD5)Approved for entry into archive by Faget Cecilia (lfaget@fcien.edu.uy) on 2023-07-31T14:39:37Z (GMT) No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.1016jjmrt.202204096.pdf: 4557826 bytes, checksum: 4fdb91b90493c84f72eed099fe081737 (MD5)Made available in DSpace by Luna Fabiana (fabiana.luna@seciu.edu.uy) on 2023-07-31T14:59:48Z (GMT). No. of bitstreams: 2 license_rdf: 19875 bytes, checksum: 9fdbed07f52437945402c4e70fa4773e (MD5) 10.1016jjmrt.202204096.pdf: 4557826 bytes, checksum: 4fdb91b90493c84f72eed099fe081737 (MD5) Previous issue date: 202215 h.application/pdfen_USengElsevier B.VJournal of Materials Research and Technology, 2022, 18:4940-5004.Las obras depositadas en el Repositorio se rigen por la Ordenanza de los Derechos de la Propiedad Intelectual de la Universidad de la República.(Res. Nº 91 de C.D.C. de 8/III/1994 – D.O. 7/IV/1994) y por la Ordenanza del Repositorio Abierto de la Universidad de la República (Res. Nº 16 de C.D.C. de 07/10/2014)info:eu-repo/semantics/openAccessLicencia Creative Commons Atribución (CC - By 4.0)Ni-Ti alloyUltrasonic characterizationMartensitic transformationsCryogenic temperatureThermal propertiesExperimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloysArtículoinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionreponame:COLIBRIinstname:Universidad de la Repúblicainstacron:Universidad de la RepúblicaMoreno-Gobbi, ArielSilva, Paulo Sergio Jr.Nespeque Correa, Diego RafaelMasó Milá, AlfredoMuños Chaves, Javier AndrésGrandini, Carlos RobertoSantos, Rafael Formenton Macedo dosMoreira Afonso, Conrado RamosLICENSElicense.txtlicense.txttext/plain; charset=utf-84267http://localhost:8080/xmlui/bitstream/20.500.12008/38531/5/license.txt6429389a7df7277b72b7924fdc7d47a9MD55CC-LICENSElicense_urllicense_urltext/plain; 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- Universidad de la Repúblicafalse
spellingShingle Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
Moreno-Gobbi, Ariel
Ni-Ti alloy
Ultrasonic characterization
Martensitic transformations
Cryogenic temperature
Thermal properties
status_str publishedVersion
title Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
title_full Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
title_fullStr Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
title_full_unstemmed Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
title_short Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
title_sort Experimental assessment of low-temperature martensite transformations in Ni-rich polycrystalline Ni-Ti alloys
topic Ni-Ti alloy
Ultrasonic characterization
Martensitic transformations
Cryogenic temperature
Thermal properties
url https://hdl.handle.net/20.500.12008/38531